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Beilstein J. Nanotechnol. 2018, 9, 3053–3068, doi:10.3762/bjnano.9.284
Figure 1: Chemical structure of OCPS (C56H96N8O36Si8).
Scheme 1: Synthesis of OCPS.
Figure 2: (a) 1H NMR, (b) 13C NMR and (c) 29Si NMR spectra of OAPS and OCPS.
Figure 3: (a) MALDI-TOF-MS spectra, (b) XRD patterns and (c) FTIR spectra of OAPS and OCPS; (d) SEM images of...
Scheme 2: Schematic diagram of the synthesis of OLDH.
Figure 4: FTIR spectra of NLDH and OLDH.
Figure 5: XPS spectra of OCPS, NLDH and OLDH.
Figure 6: (a) XRD patterns (WAXS: 5–70°, SAXS: 1–10°) and (b) crystallite size (thickness in the normal direc...
Figure 7: (a) Possible crystallographic structure of OLDH; (b) Energy-minimized molecule structure of an OCPS...
Figure 8: TEM images of (a, b) NLDH and (c, d) OLDH.
Figure 9: SEM images of (a) NLDH and (b) OLDH.
Figure 10: TG and DTG curves in (a) N2 and (b) air.
Figure 11: (a, b) Typical conversion curves at different heating rates and (c, d) plots of log(β) as a functio...
Figure 12: SEM morphology of char residues at 800 °C.
Figure 13: XPS measurements of surface components before and after thermal degradation of (a) OCPS, (b) NLDH a...
Figure 14: HRR curves of DBS-LDH adapted from [21] and OLDH.